The review highlights a variety of analytical techniques such as titrimetric, chromatographic, spectroscopic, electrophoretic, and electrochemical and their corresponding methods that have been applied in the analysis of pharmaceuticals. This review highlights the role of the analytical instrumentation and the analytical methods in assessing the quality of the drugs. Updated annually, the British Pharmacopoeia (BP). All Europoean Pharmacopoeial texts included. For this analytical instrumentation and methods play an important role. New, legally enforced standards, available from 1 August 2019. These pharmaceuticals may develop impurities at various stages of their development, transportation and storage which makes the pharmaceutical risky to be administered thus they must be detected and quantitated. To make drugs serve their purpose various chemical and instrumental methods were developed at regular intervals which are involved in the estimation of drugs. These pharmaceuticals would serve their intent only if they are free from impurities and are administered in an appropriate amount. The development of the pharmaceuticals brought a revolution in human health.
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